Before the monograph "Diamond Theory" was distributed in 1976,
two (at least) notable figures were published that illustrate
symmetry properties of the 4×4 square:
Hudson in 1905 —
Golomb in 1967 —
It is also likely that some figures illustrating Walsh functions as
two-color square arrays were published prior to 1976.
Update of Dec. 7, 2016 —
The earlier 1950's diagrams of Veitch and Karnaugh used the
1's and 0's of Boole, not those of Galois.